GCMS calibration table, January 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ JANI502\27288FB.D Vial: 21 Acq On : 16 Jan 2002 6:31 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 3.04 ug/1 623248 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pentane, /3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 262 (7,447 min): 27288FB.D (-) m/z 73.00 100.00% 73

5000 43 • < 1 ■ • * ‘ i < * • • i • < • i ‘ * 7.20 7.40 7.60 7.80 38 1, I 50 5,5, . 67, । , 87 103 ' ' i ■ ■ ■ 1 1 ' 1 1 ' I 1 TIII ' 1 1 1 ' i ■ ■ I''1 1 1 I 1 m/z 43.00 32.48% Wz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73

5000 T|-rri i }4 i i rj-T UL i ’ 7.20 7.40 7.60 7.80 45 m/z 41.05 12.21% 53 59 15 ' i ■ ■ • • i • ■ ■ ■ i 1 1 -IIPT ,............. 88.............................. ■ ■ i ■ m/z-> 10 20 _ 30 40 50 60 70 80 90 100 110 Abundance 29, 3mmom . r hy 30 MPym Tm ?’ ii Ipaaampi i 'i' 7.20 7.40 7.60 7.80 5000 rn/z 44.95 11.81%

15 41 55 70 87 ■ • i ' ■ ‘ ■ i ■ ■ ■ 1 i ■ ■ ‘ ■ i 1 ■ ' 1 i 1 ■ ■ 1 i 1 ■ ■ ■ i ■ ‘ ■ ■ i ' • ■ ' i ■ ■ ' 1 i ■ • ■ ■ i ■ m/z-> 10__ 20__ 30_ 40 50 60 70 80 90 100__ 110 Abundance #292: N-Ethylformamide ......... — 30 7.20 7.40 7.60 7.80 73 m/z 5000 44 58

! miz-> 1111s..... 10 20 --- 30 40 50 i ■ ■ ■ ■ i ■ 1 ■ ■ i 1 1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ' i ■ 60 70 80 90 100 110 7.20 7.40 7.60 7.80

27288FB.D GCMS1126.M Mon Feb 04 14:59:43 2002 Page 1

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