GCMS analysis results for sample AE00009, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\9.D Vial: 11 Acq On : 24 Jan 2002 10:52 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.58 0.39 ug/1 136580 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 38 2 1H-Azonine, octahydro- 127 C8H17N 005661-71-2 5 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 4 2-Butyne-1,4-diol, diacetate 170 C8H10O4 001573-17-7 4 Abundance Scan 276 (7.577 min): 9.D (-) m/z 4 .00 100.00% i 43

5000

83 ’ 97 mi 127 7.20 7.40 7.60 7.80 8.00 36 49 61 । |-i । - ।Ili.i II m/z-> 10 20 30 T-W TTT 1,4-— ........... 70 80 vn। i . 11103 i i 90 i-1 ■ > ■ 100 110 120 130 m/z 126.90 10.67% 40 50 60 Abundance #12247: 2-Propanone, 1,1,1-trichloro- 43

.................. ..... - 5000 7.20 7.40 7.60 7.80 8.00 m/z 46.90 9.11% I 15 I 35 49 85 97 ii7 125

MMpapbl "ww ' i ' ' ' ■ i ' ' ' ' i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #4790: 1H-Azoriine. octahydro- 30 56 7.20 7.40 7.60 7.80 8.00 70 5000 m/z 82:85 8.14% 42 127 84 1 98 . ..... 1.......... . 1 11 112 , . m/z-> Abundance ' ■ i ' ■ ' ' i ' ' 10 20 30 40

43 50 60 70 80 #4732: N-Acetylpyrrolidone 90 100 110 120 130 Il.... Illi..... 7.20 7.40 7.60 7.80 8.00 m/z 124.95 7.86% 5000- 99 127 56; 86 30 —

m/z-> 10 20 30 40 ‘ I‘* 50 ... 60 9?70....80 ......J100.. 110112 120 90 | 130 7.20 7.40 7.60 7.80 8.00

9.D GCMS0208.M Fri Feb 08 13:44:44 2002 Page 2

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