GCMS analysis results for sample AE00008, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\8.D Vial: 10 Acq On : 24 Jan 2002 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.43 3.44 ug/1 957984 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 33 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance Scan 260 (7.432 min): 8.D (-) m/z 73.00 1 00.00% I 73

5000 43

87 103 7.00 7.20 7.40 7.60 7.80 38 |, | 50 55. 61 67, । i ' ■ ■ ■ i ■ ■ ' ■ i I ri 1 ''i ■ • • • r ■I—i—<—। । । Pi । । । , , । . । . m/z 43.0,0 33.44% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.00 7.20 7.40 7.60 7.80 55 m/ z 41.05 12.27% 45 87 27 I , 39, 1 'i1 ■ ■ • । m/z-> i ' ■ ' ' i ' ' ' ■ i 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73 I 1 ' 1 1 1 ' —PPPPPP 7.00 7.20 7.40 7.60 7.80 5000 m/ z 45.05 12.21% 45

..... 2733 39 155.... ■............ m/z->_____ 10 20 30 40 50 60 70 -80 90 100 110 'Abundance #845: Silane, tetramethyl- i ' ■ ■ ■ r1 ■ ■ ■ i ■ ■ 73 7.00 7.20 7.40 7.60 7.80 m/z 71.0.0 6.97% 5000

45 15 31 1 55 .... 88............ i ■ ■ • ■ i ■ ■ ■ > i' > '-l I..... ''''I ' ’ I ‘ TrPi । f । । । । । । i-i t-|-1 । m/z-S 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

8 .D GCMS0208.M Fri Feb 08 13:42:57 2002 Page 1

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