GCMS analysis results for sample AE00007, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\7.D Vial: 6 Acq On : 24 Jan 2002 5:57 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 •MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.43 2.83 ug/1 889438 1,4-Dichlorobenzene-d4 11.48

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 33 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Pentane/3-methoxy- 102 C6H140 036839-67-5 9 4 Silane,( tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 260 (7.435 min): 7.D (-) m/ z 73.0.0 100.00% 73

5000 43

87 103 7.00 7.20 7.40 7.60 7.80 I, | 50 55. 60 67,| 38xdRmCRRmmFTndng m/z 43.00 33.80% miz->10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000- TI"T 7.00 7.20 7.40 7.60 7.80 55 m/ z 45.05 12.40% 45 87 27 39, i ■ ■ i • ■ ■ ■ i I , .......... .................. I ■ ‘ I ' i 1 ■ 1 ■ i 1 i ■ • ■ ■ i • ■ ■ ■ i ' ■ ' ' i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30 um 7.00 7.20 7.40 7.60 7.80 5000 m/z 41.00 12.01%

15 , | 41 55 70 87 i ' ’ ' ■ I ■ । • ■ ■ ■ । ■ ■ ■ ■ । ■ 1 ■ • i ■ ■ ■ ■ i ■ ■ ■ ■ I ■ ,m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- ■ । ; i . Anmn T । > 73 7.00 7.20 7.40 7.60 7.80 m/z 71.0,0 6.97% 5000 45 I

i ' ' ' 27 33 39 ' i 1 ■ ‘ ■ i ■ ' ■ ■ i 1 55 ' ' ■ i ■ ■ ■ ■ i ' ' ■ r1 ‘ ' । ■ ■ ■ 1 । ' ' ■ ■ । ' 1 1 ■ । 1 I'1"1 1 1 OTrri > itiTTiti i i miz-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

7.D GCMS0208.M FriFeb 08 13:41:13 2002 Page 1

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