GCMS analysis results for sample AD31461, Feb 11, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI602\31461.D Vial: 29 Acq On : 17 Jan 2002 4:00 pm Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.19 0.42 ug/1 96982 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propa: , 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 2-Propanol, 1,1’-[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 50 3 2-Propanol, 1,1' -oxybis- 134 C6H14O3 000110-98-5 50 4 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 45 Abundance Scan 669 (11.189 min): 31461.D(-) m/z 59.05 100.00% ,• 59 45 5000 73 103 My 10.80 11.00 11.20 11.40 11.60

miz-> 20 ■ i ■ ■ ■ ■ i • ■ 30 451 40 50 44 60 70 80 90 । l ■ ■ ■ TTT 100 110 I 120 130 m/z 45.05 56.13%

VN Abundance #9238:2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 103 ■ i ‘ • i ‘ ■ i ■ • • ■ i ■ ■ ■ • i ■ ' 45 73 10.80 11.00 11.20 11.40 11.60 31 m/z 103.05. 31.05% ---T ■'I " " i' 130 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #20830: 2-Propanol, 1.1*[(1-methyl-1.2-ethanedtyt0(oxys 59

10.80 11.00 11.20 11.40 11.60 5000 m/z 41.00 29.15%

miz-> Abundance 31

■ । ■ • ■ ■ । ■ 20 30

31 91 50 40 45

45 73

#6087:2-Propanol, 1,1‘-oxybis- 103

■ i ■ ■ ■ ■ i • ' ■ ■ i ■ ■ ■ ■ i ■ ' ■ ' i ■ ■ ' ' i • ■ ■ ‘ i ■ 1 1 • i ■ • 1 ■ i • ■ 60 59 70 80 90 100 110 117 120 130 —TIndTDenga 10.80 11.00 11.20 11.40 11.60 m/ z U 5000 103 89 72 ■ i 1 ■ ■ • i 1 • ' ■ i 1 11+Ht • i ‘ I • i ' ' ‘ ■ i ■ ■ ■ ‘ i Tr T-j-r-r-r-r-p-r miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 10.80 11.00 11.20 11.40 11.60

31461.D GCMS0103.M Thu Feb 07 12:38:42 2002 Page 2

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