GCMS unknown compounds report, sample AD31459, Feb 2002

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Laboratory report for DEP sample AD31459 identifying unknown compounds and surrogate recovery results from February 13, 2002.

NYC-WTC_000016533–000016542

Folder label: “GCMS X 12/31/01 A 1/18/02”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\JAN1602\31459.D Vial: 15 Acq On : 17 Jan 2002 1:19 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.27 0.32 ug/1 87931 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol/1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 50 2 Ethane, 1-ethoxy-1-methoxy- 104 C5H1202 010471-14-4 50 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 4 2-Propanol, 1,1‘-oxybis- 134 C6H14O3 000110-98-5 40 Abundance Scan 678 (11.272 min): 31459.D (-) m/z i 59 45 5000 73 103 ■ * i ■ ‘

m/z-> ■ I ■ “ • 1 I ■ 1 20 30 +l -51+4——++ 39 .

40 50 60 70 80 । 90 86 ■ i ■ ■ । 100 110 ।r * .paaagogoohog 120 130 m/z 11.00 11.20 11.40 11.60 44.95 61.81% Abundance #9238:2-Propanol, 1-(2-methaxy-1-methylethoxy) 59

5000 103 45 11.00 11.20 11.40 11.60 73 31 m/z 73.00 3.66% 130 । ■ ।•1 ■ i‘ • ■ ■ i1 TT1 IT N—— PT 1 I ‘ ' I 1 ' ■ -T’ ' I ' ‘ ‘ ‘ i ‘ 1 ‘ ' i 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance 45 #1926: Ethane, 1-ethxy-1-metoxy 59 _M 11.00 11.20 11.40 11.60 5000 m/z 103.05 32.24% 73 89 27 103 1 ! 1 1 ' 'T' 11 r1 1 1 ' ' 1 1 ' 1 1 11 1 1 1 1 ‘ 1 i ' ‘ 1 ' I ‘ ‘ ‘ I 1 ‘ ‘ 1 I ' ‘ 1 ' I ' 1 ‘ ‘ 1 1 ' m/z-> 20 30 40 50 60 ___ 70 80 90 100 110 120 130 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- ■ 59 11.00 11.20 11.40 11.60 ) m/z 41.05 4.35% 5000 31 45 103

89 —4—1 ‘ i 1 75 ■ 1 ' i ■ ■ ■ ■ i • ■ ■ • i1 1 ■ ‘ i ■ • ' ■ i ■ ■ ■ ■ i • 1 MMA,MMAAM) ATi । r. ■ pa i . <| i ■ m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

31459.D GCMS0103.M Thu Feb 07 09:30:23 2002 Page 2

N YC-WTC_000016541

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