NYC-WTC_000018048
Laboratory report documenting GCMS analysis of sample AD31407 conducted on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 10 pages
GCMS unknown compounds report, sample AD31459, Feb 2002
Machine-extracted title · confidence 95%Laboratory report for DEP sample AD31459 identifying unknown compounds and surrogate recovery results from February 13, 2002.
NYC-WTC_000016533–000016542Folder label: “GCMS X 12/31/01 A 1/18/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN1602\31459.D Vial: 15 Acq On : 17 Jan 2002 1:19 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
7.44 4.18 ug/1 1132140 1,4-Dichlorobenzene-d4 11.50
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 Abundance Scan 261 (7.444 mln): 31459.D (-) 73 m/ z 73.0,0 *100.00%
5000 43
38.1,1.1 67, । . 87 103 7.20 7.40 7.80 7.80 1 i ■ ' ■ ■ i 1 Tutt r111 ■ 50 11161 r1 55, 11 ■ 11 I' 1 i ' I 1 1 1 "I i *> ■ । i i > m/z 43.05 32.74% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73
5000 ■ • i 1 ■ ■ ' r1 ' 1 ' i 117 1 1 1 ’ 7.20 7.40 7.60 7.80 55 m/z " 12.25% 45 87 27 39, ; | **I****1****I***1*/a/a/a/I/B"+/I/4/4/—/tII 1 • ' i ■ ■ ' 1 1 1 ' 1 ' I ' 1 ‘ ‘ I ‘ 1 m/z-> __ 10____20___ 30 40 50 60 70 80 90 100 110 Abundance #52902 Sist c. tetrametyi- 73 1 . I mr l . , I I [T I 'I I I 7.20 7.40 7.60 7.80 5000 m/z 41.05 11.70%
45 15 53 59 88 i •1*1***1*1****E444*14A*1A**I‘AAIIIIIIIIIIIII miz-> 10__20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- rrgepmm-TrTgmu 30 7.20 n 7.40 “ ‘ 7.60 7.80 m/z 71.00 6.81% 5000
15 41 55 70 87 » • । • i • > i I'. । ■ Ji1: I । ■ l 1 1 i • 1 ■ ■ I ‘ ‘ 1i ‘ 1 -T' > I * ■ • T | I > I I | I I ‘ • ITT r . , . . . IIIr ’ । । । i m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80
31459.D GCMS0103.M Thu Feb 07 09:30:18 2002 Page 1 NYC-WTC_000016540
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NYC-WTC_000016540Source: NYC Law Department, mirrored locally
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