GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI802\31505.D Vial: 14 Acq On : 19 Jan 2002 4:17 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.05 ug/1 977437 1,4-Dichlorobenzene-d4 11.50

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol J 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1-Butanamine, 3-methyl-___ __ 87 C5H13N 000107-85-7 7 Abundance Scan 262 (7.452 mln): 31505.D (-) m/z 73.00 100.00%l 73

5000 43 —1133 87 103 7.20 7.40 7.60 7.80

miz-> ■ 1 i • ‘ 10 ‘ I ■ ■ ■ ■ i 1 20 30 +3841 40 4950—55,6057+1 60 70 I, 80 90 100 110 m/z 43.05 33.68 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 ' 1 1 ’ 1 1 "93 f ' 1 1 I 1 ‘T"'1 | ’■ ‘ 7.20 7.40 7.60 7.80 55 m/z 45.05 12.16% 45 87 27 1 39, | ----- ‘ ■ , ■ ■ ‘ ■ i ■ ■ ■ ■ i ■ ■ • • i ■ ■ ■ • i • • '' i ■ ‘ ' 'i * miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 462902: 1,3-Dioxela/d, 2 netryl- 73 1 1 ! '1 i~i FL’ । । TTrI > । 7.20 7.40 7.60 7.80 5000 43 m/z 41.05 11.08 58 27 87 ‘ 1 i ‘ ■ i ■ ■ • ■ i ' ■ ■ 1 i ■ ■ ' ■ i ■ ■ ■ ■ i ' ‘ ' i ■ ■ ■ ' I ■ ■ ‘ ■ i 1 ' ■ ■ i ■ 1 ■ ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- —TPPPTTTMPT 73 7.20 7.40 7.60 7.80 m/z 71.00 6.76 5000

15 31 45 55 88 • > [ • •' > • i » > > • ■ I-'t > 1 * |- I l'1 i i । •i•। . . . . । i • i • ■ • ■ i • ■ ■ • । * ■ • > । ■ . . । r. r. । , ph . । . . miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31505.D GCMS0103.M Wed Feb 06 15:39:26 2002 Page 1

NYC-WTC_000016653