GCMS blank analysis for sample AE00005, Feb 8 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN2402\LB.D Vial: 3 Acq On : 24 Jan 2002 2:01 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.43 3.89 ug/1 971072 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Pentanol•3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 4 1-Butanamine, 3-methyl-_________ 87 C5H13N 000107-85-7 9 'Abundance Scan 260 (7.429 min): LB.D (-) m/z 73.00 100.00% 73

5000- 43 --- | I i t r ( i i i

87 103 7.00 7,20 7.40 7.60 7.80 3?1 I |,1 1 | 1 ■ 50i > ■ 55,60 67, 1 m/z 43.0.0 32.44% i ■ ' ‘ i ' ' 1 ' 1 1 * । ■ । 1 1 I I.. m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.00 7.20 7.40 7.60 7.80 55 m/ Z 4 1.0.5 11.91% 45 i ■ ■ ■ ■ I ' i ' ' ' ' i 27 , 39, r . . 87 I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902:1,3-Dioxolane, 2-methyl- 73 i1 1 1 । Dt n ।' 1ipnv 1111 । । 7.00 7.20 7.40 7.60 7.80 5000 43 m/z 45.0,5 11.62% 58 87 27 I i ' ‘ ' i ' ' ' ' i ■ ■ ■ ' i ' ' ' ' I ■ ' ■ ■ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 - Abundance #62932: Silane, tetramethyl- -i-|=rT*-r r f n i 73 7.00 7.20 7.40 7.60 7.80 m/z 71.00 6.18% 5000

45 15 | 53 59 |..... 88............ -| 1 111 1 I ■ ■ ■ PI i i । l i’i mprhti’) > ■ ■ i । m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

LB.D GCMS0208.M Fri Feb 08 13:45:48 2002 Page 1

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