NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN2 4 02\LB.D Vial: 3
Acq On 24’Jan 2002 2:01 pm Operator: 209 GALOS
Sample GC/MS SCAN 1/3 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title 209 625/TCLP calibration table
Library C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
14.13 0.93 ug/1 295096 Naphthalene-d8 15.08
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50
2 N-(Trifluoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 43
3 Benzoic acid, 2-[(trimethylsilyl )ox 282 C13H2203Si2 003789-85-3 37
4 Benzoic 'acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37
Abundance Scan 990 (14.130 min): LB.D (-) m/z 73.00 100.00%
73
5000
267
355
45 13.80 14.00 14.20 14.40
1 103 133154 193 223 .
- —T———mmmor 323 .
m/z 266.90 34.48%
miz-> 50 100 150 200 250 300 350 400 450
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 \
5000- TT
13.80 14.00 14.20 14.40
m/z 355.05 25.96%
.............................. 207 323 |
b
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #58326: N-{Trifluoroacety!)-0.O,0"-tris(trmneihylsilyh)no
73
355 13.80 14.00 14.20 14.40
5000 m/z 267.90 9.61%
45
■ 126147 193 265 ....... I 376 ........ 481
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi \
‘I
73 267 13.80 14.00 14.20 14.40
m/z 356.05 9.00%
! 5000-
135
47
TT
7I 123 ( 233 ......... /..........
m/z~> 50 100 150 200 250 300 350 400 450 13.80 14.00 14.20 14.40
LB.D GCMS0208.M Fri Feb 08 13:45:53 2002 Page 2
NYC-WTC_000050086
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