GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1802\31505.D Vial: 14 Acq On : 19 Jan 2002 4:17 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Anthracene-dlO- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

24.92 0.22 ug/1 63986 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 2 Phenanth: ne-d10 777 188 C14D10 188 C14D10 001719-06-8 001517-22-2 91 91 3 Pentacyd 1o[8. 4.0.0(3,7) .0(4,14) .0(6 188 C14H20 000000-00-0 36 4 3H-Pyraz;ol-3-one, 2,4-dihydro-4,4-d 188 C11H12N2O 017694-06-3 33 Abundance / Scan 2165 (24.922 mln): 31505.D (-) m/z 188.10 100.00% 1(18

5000

40 52 66 80 84108 160 | 24.60 24.80 25.00 25.20 ‘ TT — m/z 184.10 14.83% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d 10- 188

5000 24.60 24.80 25.00 25.20 1 „„ 80 94 160 , m/z 79.95 13.93% -- -------- Wz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance *1906 pl, anthene-n10 188

24.60 24.80 25.00 25.20 5000 m/z 189.10 13.76% 88 80 94 160 00 —PPPmmppmmmmmmmmmmmmmmmmmpp m/z- > 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19959: Pentacyclo(8.4.0.0(3>7).0(4,14).0(6.11)]tetradecane . rr r-i i । i i i । । 188 24,60 24.80 25.00 25.20 m/z 94.00 13.41% 5000 79 92 106 117 131 145 159 173 — — | “ I" ■11 ■ ■ i ■ ■ i “ ■■I■■ “ i T’T m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.60 24.80 25.00 25.20

31505.D GCMS0103.M Wed Feb 06 15:39:31 2002 Page 2

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