GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JANI802\31505.D Vial: 14 Acq On : 19 Jan 2002 4:17 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,2-Benzenedicarboxylic acid, Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.10 0.33 ug/1 71514 Chrysene-dl2 32.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 12-Benzenedicarboxylicacid, 3-nit 211 C8H5NO6 000603-11-2 80 (2 Bis (?- ethylhexyl) phthalate 390 C24H3804 000117-81-7 56 3 Dibut alate 278 C16H2204 000084-74-2 43 4 1,2-Benzenedicarboxylic acid, mono( 278 C16H2204 004376-20-9 42 Abundance Scan 3056 (33.102 min): 31505.D (-) m/z 149.00 100.00% 149

5000 , 57 71 43 167 oq 104 32.80 33.00 33.20 33.40 S3 I 120 | 208 240 279 — ■ 14 11 A mh. 111111 rl 1* • i ■ • ■ < i ■ i • ■ । • • • • । । ■ i • > ■ • i • m/z 57.0,0 32.92% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513:1,2-Benzenedicarboxylicacid, 3-nitro- 149

I 5000 32.80 33.00 33.20 33.40 167 71 m/z 167.0,0 28.44% | 83 113 132 i| ------ ' 1 ■ i 1 ' ■ ' i ' ■ ■ ■ I ■ ■ ' 1 I ' 1 ■ ■ i ■ ■ ' 1 i ' ‘ ■ i ' ■ ■ ‘ i ■ 1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53128, 2c/2-etmahexh prthalaro 149

32.80 33.00 33.20 33.40 5000 m/z 71.10 26.51% 57 167 71 ; 83 113 279 132 | |

AAms ; ‘ ' I ‘ ‘ ‘ ‘ I ‘ 1 • ■ i ‘ ■ ■ 1 i 1 • ‘ • i 1 • 1 • i ■ ■ 1 1 i ■ ■ ' • i ‘ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39127: Dibutyl phthalate 149 32.80 33.00 33.20 33.40 m/z 43.00 26.21% 5000

57 76 93104 121 205 223 250 278 1 ■ 1 1 ------------------- PIT 1 i ■ •' ■ i ■ 11 ■ i '1 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 32.80 33.00 33.20 33.40

31505.D GCMS0103.M Wed Feb 06 15:39:36 2002 Page 3

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