GCMS analysis results for sample AD29932, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\29962.D Vial: 11 Acq On 19 Dec 2001 1:51 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Bis(2-ethylhexyl) phthalate Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

33.29 0.37 ug/1 101077 Chrysene-dl2 33.02

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Bis(2-ethylhexyl) phthalate 390 C24H3804 000117-81-7 86 2 1,2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 000603-11-2 80 3 1,2-Benzenedicarboxylic acid, dicyc 330 C20H26O4 000084-61-7 50 4 1,2-Benzenedicarboxylic acid, bis(2 278 C16H2204 _________ 000084-69-5 47 Abundance Scan 3077 (33.292 min): 29962.D (-) m/z 149.00 100.00%| 149

5000 - 167 43 57 ,71 -----== — । — — । 83 95 . 113 33.00 33.20 33.40 33.60 —4 4 + ---H132, Tm—wTr 238 - 279 207 m/z 167.00 33.11% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53128: Bis(2-ethylhexyl) phthalate 149

5000 - 57 —A I w ■ l ■ ■ 33.00 33.20 33.40 33.60 167 71 m/z 56.95 28.93% | 83 113 279 — 132 | ■ • i ’ 1 1 1 1 1 11 + m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513: 1,2-Benzenedicarboxylicacid, 3-nitro- 149 W 33.00 33.20 33.40 33.60 5000 - m/ z 71.10 21.31% 167 71 | 83 113 132 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #46907: 1,2-Benzenedicarboxylicacid, dicyclohexyl ester AAM , (\I\N dan AA 4 149 33.00 33.20 33.40 33.60 m/z 43.0 21.27% 5000 - 31 45 57 167 71 11 84 ■ ■ i ■ ■ TT 104 122 I 209 m/z-> 60 80 100 120 140 160 180 200 220 240 260 280 33.00 33.20 33.40 33.60

29962 .D GCMS1126.M Tue Jan 15 15:27:54 2002 Page 5

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