GCMS sample analysis report for AD29929, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC1401\29928.D Vial: 46 Acq On : 16 Dec 2001 10:39 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Bis(2-ethylhexyl) phthalate Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

33.29 0.37 ug/1 83293 Chrysene-dl2 33.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual Bis (2-ethylhexyl) phthalate —3-nit 211 121,2-Benzenedicarboxylicacid, 390 C24H3804 C8H5N06 000117-81-7 90 000603-11-2 87 3 Di-n-octyl phthalate 390 C24H38O4 000117-84-0 78 4 1,2-Benzenedicarboxylic acid, diiso 390 C24H3804 ______ 027554-26-3 58 Abundance Scan 3077 (33.291 mln): 29928.D (-) m/z 149.00 100.00% 149

5000 167 57 70 41 33.00 33.20 33.40 33.60 •

miz-> 20 1 —-+4 83 । l, i11 [ । , H 40 60 80 104 121 -

100 120 140 160 180 200 220 r 238 240 260 279 t

280 m/z 167.00 33.46% Abundance #53128: Bis(2-ethylhexy!) phthalate 149

5000 ‘*11171*1111′18" 1 ' 1 1 1 57 167 33.00 33.20 33.40 33.60 71 m/z 57.00 29.54% I 83 113 279 ■ ■ I ■ A ‘ — —I 132 | ________ i ।****।* TTTTr I'1’1 TIt • i ■ ■ • ' i ■1 ■' i ■ • ■ • i ■ ■ • • i • • ■ • i ■ miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #25513:1,2-Benzenedicarboxylic acid, 3-nitro- 149 ad/k a A A. 33.00 33.20 33.40 33.60 5000 m/z 55.00 21.21%

AAA 167 71 l 183 113 132 4 l' , ।. n> ।.... ।.... (.... ।.... ।.... TTT 1 . TT I IT . . . | l t I , I ‘ I > 1 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #74172: Di-n-octyl phthalate 149 33.00 33.20 33.40 33.60 m/z 70.10 20.77% 5000 57 71 167

LL I — 83 27 113 111 TT 132 160 180' 200 ‘ 220 “240 ’ 260 279 — ------A. miz-> 20 40 60 80 100 120i 140 280 33.00 33.20 33.40 33.60

29928.D GCMS1126.M Wed Jan 30 12:44:53 2002 Page 7

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