GCMS analysis results for sample AD29519, Jan 22 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\JAN0302\29465.D Vial: 28 Acq On 4 Jan 2002 12:49 pm Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************************************************** * * * * * * Peak Number 2 1,2-Benzenedicarboxylic acid, Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.13 0.41 ug/1 63644 Chrysene-d12 32.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1,2-Benzenedicarboxylic acid, 3-nit 211 C8H5NO6 000603-11-2 86 Bis ( ethylhexyl) phthalate 390 C24H3804 000117-81-7 72 1,2.4 enzenedicarboxylic acid, diiso 390 C24H3804 027554-26-3 52 4 9-2‘,2‘-Dimethylpropanoilhydrazono 576 C30H42C12N4O3 000000-00-0 45 Abundance Scan 3060 ($3.13% min): 29465.D (-) m/z 149.00 100.00% 149 )

5000 57 167 43 70 T71"i ' ' 1 1 1 । । 1 83 104 121

miz-> —+ HHH 40 60 80 100 '1 ’ 111 120 140 11—ommmhmmm 160 180 200 220 239 240 260 279 280 32.80 33.00 33.20 33.40 m/z 167.00 31.13% Abundance #25513: 1,2-Benzenedicarboxylic acid, 3-nitro- 149

5000 T T 167 32.80 33.00 33.20 33.40 71 m/z 56.95 30.39% 183 113 132 i ■ ■ ■ ■ i • 1ktysa*s**A****14*1/ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #53128; Bis(2-ethylhexyl) phthalate 149 ATWAWA ^r), w , , MM A , 32.80 33.00 33.20 33.40 5000 m/z 43.05 22.87%

N i 57 167 71 I 83 113 279 ■ ■ i ■ vi l । i 14 1 11 i r r i rI i ] i 132 •1 ■ i ■ • ■ ‘ i ' 1 • ■ i ■ • ■ ■ i • ■ ■ ■ i ■ ■ ■ ■ i 1 ■ ■ • i • 1 • ■ i' • miz-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 #53134: 1,2-Benzenedicarboxylic acid, diisooctyl ester 149 “M M rWWis 32.80 33.00 33.20 ‘33'40 ' m/z 70.00 20.64% 5000 57 . 167 70 83 104 279 .................................................. .. 132 I ‘ 1***I* iiii i ' ■ • ■ 1 ' 1 • 1 i ■ ■ ' ■ i ■ ■ ■ 1 I ‘ 1 1 • 1 ■ • miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 32.80 33.00 33.20 33.40

29465.D GCMS0103.M Fri Jan 11 08:32:41 2002 Page 2

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