NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30605.D Vial: 30
Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********** * *********************************************************
Peak Number 11 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
30.25 0.39 ug/1 89742 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy^-, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 42
2 1,1,1,5,7>X7-Heptamethyl-3/3-bis (t 444 C13H40O5Si6 038147-00-1 32
3 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23
4 trans-3-Hexenedioic acid, bis(t r i me 288 Cl 2H2404Si2 000000-00-0 23
Abundance Scan 2745 (30.247 mln): 30605.D (-) m/z 73.0,0 100.00%
i 73
5000 147
221 ... A । /1 L । . i i >
281 355 429 30.00 30.20 30.40 30.60
m/z->
38
TTT
50
117
i *** " ■ i ■
100 150
-19144
200
. .. 327 J, 401 P
250 300 350 400 450 500 550
m/z 147.0,0 39.58%
Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trlm
73
5000 —_-----------
147 30.00 30.20 30.40 30.60
m/z 221.0 22.00%
221 281.___327L 415
i 519 561
■ ' i ■ • ■ ■ i ■ ■ ' ■ i ‘ • i ■ I ■ i 1" । । । । ।
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #56714: 1.1.1,5.7.7.7-Heptamethy-3.3-bis(trimethylsiloxy)t
73
147 30.00 30.20 30.40 30.60
5000 267 m/z 281.10 12.64%
355 429
45 . 207
Td100/mn/n/—1dmmm//m3—mnun/nnB—B—I-T
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #40777:2-Hexenedioic acid, bis(trimethylsily!) ester, (E)-
73 30.00 30.20 30.40 30.60
m/z 355.0 12.54%
5000
147
45
112 244 273
Ti " 1 ■ ■ । ।111111' » i | i » / « । i j i » । > « » i । i BIIIIIII1 TT
30.00 30.20 30.40 30.60
miz—> 50 100 150 200 250 300 350 400 450 500 550
30605.D GCMS1126.M Wed Jan 23 08:29:21 2002 Page 11
NYC-WTC_000018211
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