Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
NYC-WTC_000018174–000018193Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
30.25 0.64 ug/1 150666 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 1 -Monolinoleovlglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 38 3 2-Hexenediolc acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23 4 1,1,1,5. ^7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 23 Abundance 1 Scan 2746 (30.252 mln): 30714.D (-) m/z 73.00 100.00% 73
5000 147 221 281 355 4k, 325,4. .4014?%. 45 30.00 30.20 30.40 30.60 TTIT .. . m/z 147.00 38.50% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tfs(trim 73
5000 • • i • • 147 30.00 30.20 30.40 30.60 221 281 rn/z 221.0,5 19.91% 327 415 519 561 ‘ ‘ i 1 ■ ‘ • i ‘ ‘ • i ■ ■ ■ ■ i ■ ■^1 " ■ • i ■ • ■ 1 i 1 1 1 1 i 11 ' 1 i ' ’ m/z-> 50 100 150 200 250 350 300 400 450 500 550 Abundance #58871; 1-Moriinoleoylglycerol trimethylsilyl ether 73
. 207 30.00 30.20 30.40 30.60 5000 147 m/z 355.05 13.21% 34 103 281 ; I I 395 482 1 f ''1 1 I 1 ■ i ■ ■ ■ ■ i • 1 ■ • i 1 1 1 1 I 1 1 1 1 1 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #40777:2-Hexenedioic acid, bls(trlmethylsilyl) ester, (E)- ................... 73 30.00 30.20 30.40 30.60 I m/z 281.00 12.83% 5000 147 45
112, 244 273 ——— ■ i ■ 1 ■ ■ i ' • ' ■ i ■ ■ ■ ■ i ■ ■ • ' i ■ ■ i • ■ 1 1 1 1 1 1 ' 1 1 1 ■ ■ i ■ ' ■1 I'1111’ 1 1 1 I ' 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
30714.D GCMS1126.M Wed Jan 23 08:50:34 2002 Page 10
NYC-WTC_000018190
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NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder