NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51
Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
30.26 0.60 ug/1 129757 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1 -Monol inoleoylglyceroltrimethylsi 498 C27H54O4Si2 054284-45-6 42
2 3-Isopropoxy-1,1,1,7 ,7-hexamethyl 576 C18H5207S17 071579-69-6 40
3 1,1,1,5,7,7,7-Heptatfiiethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1 28
42-Hexenedioicacid,bis(trimethylsi288C12H2404Si2
Abundance Scan 2746 (30,256 min): 30934.D (-)
055494-10-5 17
m/z 73.00 100.00%
73
5000 147
221
i 45
281 355
. 1 . 325. I 401 1
429 30.00 30.20 30.40 30.60
I TTT । -i । 117. .
। -r * । h । +1914——
। । i"i ■ ? ’ I i i"i ’Itt i-i f rT i vr i । । i । । । r । m/z 147.00 38.63%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 * ■ i ■ ■ ‘ 4**1*3
30.00 30.20 30.40 30.60
34 103
281 m/z 221.05 22.17%
395
1 1 i ■ ■ ■ ■ i ■ 1
t i
• )•>■• r> 11nmmnnnn3
1 ■ 482
■ i ■ ‘ ' i ‘ • i • •
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503; 3-Isopropoxy-1.1.1.7.7,7-hexamethyl-3,5,5-tris(trim
73
30.00 30.20 30.40 30.60
5000
147
m/z 355.05 14.18%
221 281
111 ■ •1 ■ ।1 1 ■ ■ । • ■ • ■ । ‘ । ■1 f ■ । *
327____ 415______ 519 561
1d*nnmn0mu —ut—a1fr
miz-s 50 100 150 200 250 300 350 400 450 500 550
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t T T T
73 30.00 30.20 30.40 30.60
m/z 281.10 14.14%
147
5000 267
t 355 429
i 45 207
• ‘ I ‘ ‘ ' I • ' ' ‘ I ' ' ' * I ' ' ‘ ‘ ( 1 1 ' 1 I • ‘ f I' 1 1 ' I ‘ ( ' । ■ i' ■ ■ ■ । ■
50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 3040 30.60
30934.D GCMS1126.M Fri Jan 25 11:47:22 2002 Page 12
NYC-WTC_000018751
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