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GC/MS analysis results for sample AD30934, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.

NYC-WTC_000018733–000018753

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 28.66 0.49 ug/1 158578 Phenanthrene-dl0 24.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 33 2 3-1 sopropoxy-1,1, 1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 3 Benzoic acid, 2 -bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 27 4 Benzoic acid, 2 ,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 17 Abundance Scan 2572 (28.659 mln): 30934.D (-) m/z 73.00 1 00.00% 73

5000 147 2?1 281 355 45 191.| L 327, 1 401 429 28.40 28.60 28.80 29.00 117. , dafasst 191 1*T1 rl ' 249. miz-> Abundance "go 100 150 200 ■ I ' • ' ■ i 1 i; । ... . । । . i . । ■ . . . । . . .. । . . 250 300 350 400 450 #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 500 550 m/z 147.00 35.16%

73

5000 147 207 ............... ‘ ■ I ‘ U .... ‘ ‘ I ‘ 1' ■ ■ i • • • • i ■ 1 28.40 28.60 28.80 29.00 34 103 ; 281 m/z 221.0,5 19.42% 395 1 ' i • —* , 1,1 — ______ i , • i ■ ■ ■ ■ i 1 482 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-lsopropoxy-1.1.1.7.7,7-hexamettiyl-3,5,5-tris(trirn 73

28.40 28.60 28.80 29.00 5000 m/z 355.0,5 19.29% 147 221 281 22= 415 I l t ; 519 561 14*1**A+--*I--*+1*6**1**--1$**11I$1AI1* miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-> trimet 73 28.40 28.60 28.80 29.00 m/z 281.0,0 16.48% 5000 355 45 I ...... ....... 133 , 193 223 281.......................................... miz-> 50 100 150 200 250 300 350 400 450 500 550 ' 28.40 28.60 28.80 29.00

30934.D GCMS1126.M Fri Jan 25 11:47:17 2002 Page 11

NYC-WTC_000018750

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NYC-WTC_000018750Source: NYC Law Department, mirrored locally

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