GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

28.50 0.53 ug/1 180998 Phenanthrene-dl0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monol inoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 2 Benzoic acid, 2,5-bis (trimethylsilo 370 C16H30O4Si3 003618-20-0 37 3 3-Isopropoxy-1,1,1,7,7, 7-hexamethyl 576 C18H52O7S17 071579-69-6 28 4 Trisiloxane, 1,1,1,^,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 28 Abundance Scan 2555 (28.502 min): 27288.D (-) m/z 73.00 100.00% 73

5000 147 221 281 355 251. [ . 327 [ 28.20 28.40 28.60 28.80 i -—-pip 45 117 4 ..1914, TTTTTTuu—4011u 429 rPpmengat 111 I rn/z 147.00 34.51% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 28.20 28.40 28.60 28.80 34 103 281 m/z 355.0,5 19.86% 395 ■ r •f • ■ i ■ ■1 ■ । ■ ■ ■ ■ । ■1 ‘ ‘ 17 ‘ 482 ' I ■ • ' ‘ I ‘ ‘ ‘ 1 1 ‘ ■ 1 i ■ ■ ‘ ■ i m/z-> 5b 100 150 200 250 300 350 400 450 500 550 Abundance 473978: Benzoic acid. 2.5-bis(trimethy’slaxy) . trimsthlts 73 355 - 28.20 28.40 28.60 28.80 5000 m/z 221.05 18.74% 45 147 179 223 267 297 ■ ■ i ' ■ 1 ‘ i ■ ■ ■ • 1 1 ■ ■ ' i ' ‘ 1 ‘ i • ■ ■ ■ i 1 ■ • ■ i ' 1 ■ ■ i * ■ ■ ■ i • • ■ ■ i • ‘ ■ i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 28.20 28*40 28.60 28.80 m/z 281.0,0 15.97% 5000 147 221 281 327,Psi 415 519 ■ ।561 her panadarit.a ii ■ ' i ' • i ‘ ■ i ■ 1 • ■ i ■ ' ‘ • i ■ ■ f * i ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.20 28.40 28.60 28.80

27288.D GCMS1126.M Mon Feb 04 15:23:37 2002 Page 11

NYC-WTC_000016113