GCMS analysis results for sample AD27288, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

28.50 0.53 ug/1 180998 Phenanthrene-dl0 24.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 38 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 28 4 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 28 Abundance Scan 2555 (28.502 min): 27288.D (-) m/ z 73.00 100.00% 73

5000 147 221 281 355 191 [ 251 327 [ 401 429 28.20 28.40 28.60 28*80 im/z-> 447+ 117 1" l ean ■ ■ 50 100 150 200 1 fP r। । f i 250 300 350 i-i t |‘> i i > T i‘i t i । i i r i |' i i ri । i i

400 450 500 550 m/z 147.00 34.51% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 28.20 28.40 28.60 28.80 34 103 281 m/z 355.05 19.86% 395 I i . 482 *‘1**I** ■ ‘ i ■ • ■ ■ i • • ' ■ i 1 • • ■ i ' ■ ■ ■ i • • i • ■ ■ • i ■ ■ ■ ' i ■ ' miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73078 Benzoic add, 2.5-bis(trimethylsiioxy)- trimethyls 73 355 ...................... /........................ 28.20 28.40 28.60 28.80 5000 m/z 221.05 18.74% 45

miz-> . 147 179 , 223, | 267,297 ......... .................... 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 28.20 28.40 28.60 28.80 m/z 281.00 15.97%

5000 147 221 281 327 415 I I i , 519 561 ■ ■ i ' ' ‘ ■ i ■ ■ ' • i ■ ' ■ ' i • 1 • ' i 1 ‘ r ' i ■ • ■ 1 i ■ • ■ • i ■ ■ ■ ■ i ■ • ■ • i TIT • i > • m/z~> 50 100 150 200 250 300 350 400 450 500 550 28.20 28.40 28.60 28.80

27288.D GCMS0103.M Thu Jan 10 09:37:12 2002 Page 9

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