Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
NYC-WTC_000018005–000018025Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
30.10 0.64 ug/1 146245 Chrysene-dl2 32.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-He amethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 2 Tris (trimethylsi lyl)borate 278 C9H27BO3S13 004325-85-3 12 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 12 4 3-Isopropox; 1,1,1,5,5,5-hexamethyl 354 C12H3404S14 072182-11-7 10 Abundance Scan 2729 (30.100 min): 27288.D (-) m/z 73.00 1 00.00% 73
5000 147 221 1 281 355 429 29.80 30.00 30.20 30.40 45 I mmmpt 117.. . TTHTTTT 911.251 n 11 n 11 I ...4a—327....... p 11111 n I TamB——h— 401 1 h44m**"m**2*m**1***0421*18 m/z 147.00 36.11% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 [Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 ■ > ■ | ' C. i । /i i'i । । । । । । > । i i ■ 5000 267 355 429 29.80 30.00 30.20 30.40 45 207 m/z 221.05 21.40% ’***’*t*’****’H5" ......... I..... Ton TTppDT miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #39028 Tris(trimethylsily)borate 73 221
29.80 30.00 30.20 30.40 5000 m/z 355.05 14.30% 263 133 175 i j..r.।।।..i.)....।.t.1p.1.p...fi।|¥.।।।।।.j ....।....t. m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet d-makmmamm2100ab.k.kk 73 29.80 30.00 30.20 30.40 m/z 281.00 12.84% 5000 355 45 133, 193 223 _ 281 Tpmmmmpmmpmppmmpmpe prrrpTTTpTTTpTrTTT miz—> 40 60 80 100120140160180200220240260280300320340360380400420 • ‘ i ‘ ' 1 • i ‘ 1 ' • i ■ • ■ ' i ' ‘ 29.80 30.00 30.20 30.40
27288.D GCMS0103.M Thu Jan 10 09:37:17 2002 Page 10
NYC-WTC_000018022
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NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017980
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000017981
Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.
Filed in the same folder
NYC-WTC_000017989
Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.
Filed in the same folder
NYC-WTC_000017997
Laboratory report noting detection of 1,1,2,2-Tetrachloroethane in a water sample with no other non-target compounds.
Filed in the same folder
NYC-WTC_000018026
Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.
Filed in the same folder