Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
NYC-WTC_000018155–000018173Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30713.D Vial: 28 Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
30.25 0.47 ug/1 123012 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 34 2 3-Isopropoxy-1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 3 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 17 4 SilanamineT N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 16 Abundance Scan 2745 (30.247 mln): 30713.D (-) m/z 72.95 100.00% 73
5000 147 221 281 355 220 TTTu 1171 1 30.00 30.20 30.40 30.60 i miz-> 45 1*11 I* 50 117 , 100 +1911-—8241019 150 200 250 300 350 400 450 500 550 m/z 147.00 34.50% Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 147 . . . । ■'I c i f . r, . । . > . > । . 5000 267 30.00 30.20 30.40 30.60 355 429 45 207 m/z 221.05 17.39% * * i 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1.1.1.7.7.7-hexamethyl-3,5,5-tris(trim 73 —- 30.00 30.20 30.40 30.60 5000- m/z 281.00 11.79% 147 221 281 327 415 519 561 • 1 i i ' ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ 1 ■ 1 1 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56734:3-Trimethylsilyloxystearic acid, trimethylsilyl est ■ • i • ■ ■ ■ i ■ • ■ ■ i ■ ■ ■ • i • ' 73 30.00 30.20 30.40 30.60 m/z 355.0 11.03% 5000 147 233
313 429 . [ f .. I I I I I I 189 [■ ■ '■339 387 [ ■ ■ i ■ ■ ‘ ‘ । • ■ • ■ । li ■ l ■1 1 ■ ■ ■ ■ । ■ • • • । • 1 i ■ ■ ■ '■ i •' ■ ‘ ■ i ■ ■ ‘ • i ' ■ • ‘ i ‘ ■
miz-> 50 100 150 200 250 300I 350 400 450 500 550 30.00 30.20 30.40 30.60
30713.D GCMS1126.M Wed Jan 23 08:47:02 2002 Page 10
NYC-WTC_000018171
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NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder