NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30705.D Vial: 46
Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 11 3-1sopropoxy-1,1,1,7,7,7-hexam Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
31.71 0.49 ug/1 97225 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32
2 Mercaptoacetic acid, bis(trimethyls 236 C8H20O2SSi2 006398-62-5 22
3 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 11
4 Methyl bis (p-chlorgiphenyl) acetate 294 C15H12C12O2 005359-38-6 10
Abundance Scan/2905 (31.710 min): 30705.D (-) m/ z 73.00 100.00%
73
5000
147
221 t---
12" f
38
—H 117
’I i " " j 7611246 211,325 355...
f T "0" j"rf II i i-i f ।-j i i j । i
429 31.40 31.60 31.80 32.00
m/z 147.10 35.63%
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
5000 T
/ \ T 7
147 31.40 31.60 31.80 32.00
m/z 221.05 22.21%
. 415, .519561
miz-> ' 5o' ' 100 ' 150 ‘ ' 200 250 ‘ ‘ 300 ' 350 ' ‘ 400 450 500 550 '
Abundance #30949: Mercaptoace tic acid, bis(trimethylsilyl)-
73 147
31.40 31.60 31.80 32.00
5000 m/z 234.95 19.27%
221
45
104. I 193
■ 'I ir
miz-> 50 100 150 200 250 300 350 400 450 500 550 ‘
Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy] —■ 1 ■ i ■ • ■ ■ i 1 • • ' 1 1 1 1 1 i 1 1 1 1 I
73 31.40 31.60 31.80 32.00
281 m/z 236.95 12.54%
209
5000 45 251
. 179
■ ■ i ■ ■
—120lane
147 I
1 ■ i • ' 1 ■ i ■ ■ ■ ■ i 1 ' ■ ■ i 1 ' • ‘ i ' • ‘ ■ i ■ • ' ■ i ■ ■ ■ • i ‘ 1 ' ■ i ■ 1 ' • i ■ ■ ■ ■ i
miz-> 50 100 150 200 250 300 350 400 450 500 550 31.40 31.60 31.80 32.00
30705.D GCMS1126.M Fri Jan 25 11:27:43 2002 Page 11
NYC-WTC_000018622
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