NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30705.D Vial: 46
Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 10 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
30.25 0.46 ug/1 90416 Chrysene-dl2 33.02
Hit# of 5 Tent at iveID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1/7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40
2 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25
3 2-Hexenedioic acid, bis(trimethylsi 288 C12H2404Si2 055494-10-5 23
4 Butanoic acid f/3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23
Abundance (7 Scan 2746 (30.250 min): 30705.D (-) m/ z 73.00 1 00.00%
73
5000 147
221 —’’O3931’7’-*I8**
281 355 429 30.00 30.20 30.40 30.60
miz->
45
50
117 ,
ff J l 'i f 1111
100 150
191----4438741401
200 250 300 350 400 450 500 550
m/z 147.00 41.02%
Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73
! 5000 r 1- 14 ■ * * i * *
147 30.00 30.20 30.40 30.60
221 281
m/z 221.05 21.38%
I
miz->
■ ■ i ■ ■ • • i 1 ■ ■ ■ i 1 ■ ■ • i '
50 100 150 200 250 300 350 400 450 500
327—41-51 550 561
11' ■
Abundance #56714: 1,1.1.5.7.7.7-Heptamethyl-3.3-bis(trimethysiloxy)t
i 73
mpumemmatri
30.00 30.20 30.40 30.60
147
5000 267 m/z 355.05 14.77%
355 429
45 207
11,......... ........................... .............. .. .......................... ..
miz->
Abundance
50 100 150 200 250 300 350
#40777:2-Hexenedioic add, bis(trimethylsilyl) ester, (E)-
400 450 500 550
........ l\.........
30.00 30.20 30.40 30.60
73
m/z 281.00 13.04%
5000
147
45
m/z->
,
50
1112
100
244 273
• ■ I ■ ' ■ ■ i • • ■ •' i ■ ‘ 1 ■ i ■ ' 1 ■ i ' ' ‘ ■ i ■ ■ ' ' i 1 ■ ‘ ■ i ■ 1 ' 1 i ‘ •
150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
30705.D GCMS1126.M Fri Jan 25 11:27:38 2002 Page 10
NYC-WTC_000018621
OCR can misread numbers and units. Confirm readings against the page image before using them.