Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
NYC-WTC_000018605–000018623Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30705.D Vial: 46 Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
28.65 0.33 ug/1 101462 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 40 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 3 3-1sopropoxy- 1,1, 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 33 4 N-Methyladren line, tri-TMS 413 C19H39NO3Si3 000000-00-0 17 Abundance ' Scan 2572 (28.653 mln): 30705.D (-) m/z 73.0,0 100.00% 73
5000 147 . . 1 . . i rf i — । । । r-| । । 221 281 355 45 117 . ..................... 1.. 327 1 401 429 28.40 28.60 28.80 29.00 TTT 1—* . f । > । । । i i । । i । । । । । । m/z 147.00 30.95% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000 , ........ / \.................. 28.40 28.60 28.80 29.00 369 m/z 221.05 18.54% 207 249 338 I rn/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975; Benzoic acid, 2.4-bis[(trimethylsilyl)oxy]- trimet 713 ............ /.................... 1 1 I ‘ ‘ ‘ ‘ I ‘ ‘ ‘ 1 1 1 ' ' 28.40 28.60 28.80 29.00 5000 355 m/z 355.0 17.66% 45 133 193 223 281______ |__________________ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1.1,7,7,7-hexamethyl-3,5,5-tris(trim . ................. ,............. i 73 2840 28.60 28.80 29.00 l m/z 281.00 16.48% 5000 147
.... ..0000...21.,.21,.827—...1 415 .58581 I « । 18s » p । । j j । < n । i r m/z-> 50 100 150 200 250 300 350 400 450 500 550 28.40 28.60 28.80 29.00
30705.D GCMS1126.M Fri Jan 25 11:27:34 2002 Page 9
NYC-WTC_000018620
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder