Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
NYC-WTC_000018754–000018774Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
28.65 0.49 ug/1 175665 Phenanthrene-dl0 24.98
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 2 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 30 3 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 25 4 Benzoic acid, 2, bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 16 Abundance 5 2572 (28.654 mln): 30935.D (-) m/z 73.00 100.00% 73
5000 147 r • -1 . • 1 . r ... 355 1 miz-> (Abundance 45 1***4 1 50 ——— 100 117 PI 150 191 । 200 LX 250 300350 325, L I "l 1> I 400 #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet * I I > 401 429 f I ‘l 1 I 450 I : l 28.40 28.60 28.80 29.00 m/z 147.0,0 34.04%
73 147 281 ■r/r yr, ■ . | , 5000 T-r-|-r 28.40 28.60 28.80 29.00 369 m/z 221.05 18.77% 207 I 249.1 338!.. m/z-> 50 100 150 200 250 300 '350 400 450 Abundance #58871: 1-Monolinoleoy‘glycerol trimethylsilyl ether 73
207 28.40 28.60 28.80 29.00 5000 147 m/z 355.05 17.02% 34 103 281 i 395 482 i » » । । 11 D i ! i । । I- r r1 > । i i i r m/z-> 50 100 150 2oo‘ 250 300 350 400 450 . ..................... ,,.......................... Abundance #54808: N-Methyladrenaline, tri-TMS 73 28.40 28.60 28.80 29.00 m/z 281.00 13.84% 5000 355 45 207 267 323 _• ,‘ Li ■ ■ III.......................... I............ I ■ • । * * * * । * < • • । * » * * । * ■----- miz-> 50 100 150 200 250 300 350 400 450 28.40 28.60 28.80 29.00
30935.D GCMS1126.M Fri Jan 25 11:50:56 2002 Page 10
NYC-WTC_000018770
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
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NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder