GCMS analysis log for sample AD30712, Jan 2002

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Data File C:\HPCHEM\1\DATA\DEC3101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

28.65 1.13 ug/1 328560 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoyl erol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 Trisiloxane,1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 28 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 25 4 N-Methyladrenaline, tri-TMS 413 C19H39NO3Si3 000000-00-0 17 Abundance 7 Scan 2571 (28.650 min): 30712.D (-) m/z 73.0.0 100.00% 73

5000 147 221 281 355 • r (1 • * ‘ 14 • 191 L 249 . [ . 327, . 28.40 28.60 28.80 29.00 45 96 117 . 401 429 —T T —Pr m/z 147.00 32.99% miz-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 34 28.40 28.60 28.80 29.00 103 281 18.51% ■ ■ l 17, ■ ■ 395 482 > * I ' * ' ‘ I * 1 t-[—i—r-T—r miz-s 50 100 150 200 250 300 350 400 450 Abundance #52459: Trisiloxane, 1,1.1.5.5.5-hexamethyl-3.3-bis[(trimet 73 147 k 281 28.40 28.60 28.80 29.00 5000- m/z 355.0 15.56% t 907 369 I ............... 20., 249 J.., 338 1 miz-> 50 ' ‘ 100 ‘ ‘ 150 ‘ 200 ‘ ‘ 250 ‘ 300 ' 350 400 ' 450 Abundance #73975: Benzoic acid, 2,4-bis[(trlmethy!silyl)oxy]-, trimet 73 28.40 28.60 28.80 29.00 m/z 281.00 14.12% 5000 355 45 133 193 223 281 m/z-> --------------- 50 100 150 200 250 300 350 ’1*1* 400 450 ....... ) 1 1 i 1 ■ ■ ■ i • P 28.40 28.60 28.80 29.00

30712.D GCMS1126.M Wed Jan 23 08:43:17 2002 Page 11

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