NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 24 pages
GCMS analysis log for sample AD30712, Jan 2002
Machine-extracted title · confidence 100%Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
NYC-WTC_000018214–000018237Folder label: “GCMS X 12/27/01 A 1/16/02”
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\DEC3 101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.
30.25 1.55 ug/1 294651 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoyl glycerol trimethylsi 498 C27H5404S12 054284-45-6 42 2 Benzoic acid ,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 27 3 3-1 sopropoxy -1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Tris (trimethylsilyl)borate 278 C9H27BO3Si3 004325-85-3 14 Abundance Scan 2745 (30.248 min): 30712.D (-) m/z 72.9,5 100.00% 1 73
5000 147 221 281 355 rs30.00 rTm • ■ I ■ ■ 30.20 30.40 30.60 m/z-> 45 ■ ■ '"I 1 1 50 117 100 4,11914-251.1, .3274 412 150 200 250 300 350 400 450 500 550 m/z 147.00 36.86% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 -------PPP 30.00 30.20 30.40 30.60 34 103 । 281 m/z 221.05 21.56% 1 395, 482 miz- > 50 100 150 200 250 300 350 400 450 500 550 Abundance #73075: Benzoic acid, 2.4-bis[(trimethylsily!)oxyj-. trimet ! 73
30.00 30.20 30.40 30.60 5000 355 m/z 355.0 13.75% 45 133 193 223 281________ ___________________________
miz-> ’50 100 ’ 150 " 200 250 " 300 350 400 450 " 500 ’ 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyi-3,5,5-tris(trim T T T T 73 30.00 30.20 30.40 30.60 m/z 281.00 12.28% 5000 147
221 281 327 । . 415, ..519561 • • । • ’*1** miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
30712.D GCMS1126.M Wed Jan 23 08:43:22 2002 Page 12
NYC-WTC_000018232
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NYC-WTC_000018232Source: NYC Law Department, mirrored locally
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NYC-WTC_000036656
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