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GCMS analysis results for sample AD31074, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02

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Scanned page image, NYC-WTC_000017427
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 1-Monolinoleoylglycerol trimet Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

30.09 2.16 ug/1 488807 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 23 3 Trisilo: ane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 20 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 18 Abundance < Scan 2729 (30.094 min): 31074.D (-) m/ z 73.00 100.00% 73

5000 147 221 n-rT-r-r-r-r-r ----- 281 355 420 29.80 30.00 30.20 30.40 45 ' ■' i 1 r 96 117 249, 4. 327.., . 401 17450 250 ‘ ' SOO ' 350 ' ‘ ‘400 m/z 147.00 38.87% m/z-> 50 100 150 200 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 ■ • i ‘ ■ ■ i ■ ■ 29.80 30.00 30.20 30.40 34 103 m/z 221.05 21.79% ' I 281 I I I 395 i . 482 m/z-> __ 50 100 ‘ ' 150 ' ’ 200 250 300 350 400 450 Abundance 73 147 ■ • i ■ ■ 29.80 30.00 30.20 30.40 5000 m/z 355.05 13.97% 45 190 219 ■ ■ i ■ ■ m/z-> 50 ' 100 ' 150 ' ' 200 ' 250 300 350 400 450 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trirnet 731 147 29.80 30.00 30.20 30.40 281 m/z 281.00 13.14% 5000

369 II , ] 207 249 , L, , , 338 .. m/z-> 50 100 150 200 250 300 350 400 450 29.80 30.00 30.20 30.40

31074.D GCMS0103.M Wed Jan 09 12:25:17 2002 Page 15

NYC-WTC_0000 17427

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NYC-WTC_000017427Source: NYC Law Department, mirrored locally

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