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GCMS analysis results for sample AD30985, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018280
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC31O1\3O985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1-Monolinoleoylglycerol trimet Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 31.72 1.97 ug/1 553466 Chrysene-dl2 33.02 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 45 2 3-Isopropp5€y-l, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 34 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 16 4 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 12 Abundance Scan 2906 (31.720 mln): 30985.D (-) m/z 73.00 100.00% 73

• I 5000 147 221 **I*1*44*** 281 355 429 31.40 31.60 31.80 32.00

m/z~> 45 , II r["m the 50 -11715011 1914 100 —— 200 250 251., 1 , 327, 1 300 350 401 V 400 450 500 550 m/z 147.00 41.35% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 31.40 31.60 31.80 32.00 ‘ ‘ ' 34 103 i 281 m/z 221.05 23.95% 395 482 I i I ■ ■ ' i 1 • ■ ' i ' • **n//6//1/A//84/4/*/4*/1a*/***1**1***14a m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-Isopropoxy-1,1.1.7.7,7-hexamethui-3 5,5-tris(trim 73 _________ 1 ’ I’AIS* • * i • ■ • ■ i 31.40 31.60 31.80 32.00 5000 m/z 281.00 16.54% 147

221 281 327 415 519 561 m/z-> 50 100 150 200 250 300 350’400 450 "500 550’ Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bls[(trimet *18-188*1* I I l I « I I t j

73 147 31.40 31.60 31.80 32.00 281 m/z 355.05 11.64% 5000

369 207 249, 338 1.............. —I m/z-> 50 100 150 200 250 300 350 400 450 500 550 31.40 31.60 31.80 32.00

30985.D GCMS1126.M Wed Jan 23 08:57:56 2002 Page 12

NYC-WTC_000018280

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NYC-WTC_000018280Source: NYC Law Department, mirrored locally

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