Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
NYC-WTC_000018262–000018285Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
30.25 2.02 ug/1 568765 Chrysene-dl2 33.02
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 2 3-Isopropoxy-^fl,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 Benzoic acid; 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 16 4 Tris (trimethylsilyl) borate 278 C9H27BO3Si3 004325-85-3 10 Abundance < Scan 2746 (30.251 min): 30985.D (-) m/ z 73.00 1 00.00% 73
5000- 147 221 Tmr 281 355 429 30.00 30.20 30.40 30.60
miz-> 45 Tmm—BT 50 117 100 +1914—— 249-4.327401 500 150 200 250 300 350 400 450 * • । • ■ ■ • । 550 • m/z 147.0,0 37.92% Abundance #56714; 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
147 267 ' 1 i -r-p-n-ry-r-T 5000 30.00 30.20 30.40 30.60 355 429 45 207 m/z 221.0,5 21.98%
miz-> 50 100 150 200 250 300 350 ' 400 450 ' 500 ‘ 550 Abundance #60503; 3-sopropoxy-1.1.1.7,7.7-hexamethyl-3,5,5-tris(trim 713 -r-ryr-r 30.00 30.20 30.40 30.60 5000 147 m/z 355.0,5 14.57% 221 281 327 415 i 519 561 miz-> 50 ' 100 150 200 ‘ ’ 250 ' 300 350 ‘ ' 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 713 30.00 30.20 30.40 30.60 m/z 281.00 14.28% 5000 355 45 133, 193 223 281 vin 1. mhi ■ । .-fl A. 1 l • ‘ f • [ r ■ । "I"I I i i | r r-> r (■ i i i i j i i ■ ■ ( i 1 1 ' i ‘ 1 1 i 1 ' ’4 i 1 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 30.00 30.20 30.40 30.60
30985.D GCMS1126.M Wed Jan 23 08:57:51 2002 Page 11
NYC-WTC_000018279
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder