NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis summary, sample AD27288, Dec 2001
Machine-extracted title · confidence 100%GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
NYC-WTC_000016096–000016117Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JANO802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
30.10 0.64 ug/1 146245 Chrysene-dl2 32.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis (t 444 C13H4005Si6 038147-00-1 33 2 Tris (trimethylsilyl) borate 278 C9H27BO3S13 004325-85-3 12 3 Benzoic acid, 2,4-bis[ (trimethylsil 370 C16H30O4Si3 010586-16-0 12 4 3-Isopropoxy-1,1,1,5,^,5-hexamethyl 354 C12H3404Si4 072182-11-7 10 Abundance Scan 2729 (30.100 min): 27288.D (-) m/z 100.00% 73
5000 147 221 1 1 1 FT -+ -147 ■ ‘ i ‘ ■ 281 355 429 29.80 30.00 30.20 30.40 251........ ..... 327.' ........ 401 0 mmmm 45 m/z 147.00 36.11% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxyjt 73
147 267 TTIP—ITIT 5000 29.80 30.00 30.20 30.40 355 429 45 . 207 m/z 221.05 21.40% 1.......... i.......... I..... WPpag TTgpp m/z->__ 40 60 80 100120140160180200220240260280300320340360380400420 Abundance 34023* Tnsm • Msil st 73 221 29.80 30.00 30.20 30.40 5000 m/z 355.05 14.30% 263 133 175
miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #73975: Benzoic acid, 2,4-bis[(trimethyisilyl)oxy]-, trimet 713 29.80 30.00 30.20 30.40 m/z 281.00 12.84% 5000 355 45 133 193 223 281 TT m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 29.80 30.00 30.20 30.40
27288.D GCMS1126.M Mon Feb 04 15:23:42 2002 Page 12
NYC-WTC_000016114
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