GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

31.56 0.46 ug/1 106061 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1,1,1,7,7, Z-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Ethanedioic acid, bis rimethylsily 234 C8H1804Si2 018294-04-7 25 3 3-(3-Hydroxyphenyl) -3 -hydroxypropio 398 C18H3404Si3 000000-00-0 23 4 Tris (trimethyl silyl) borate 278 C9H27BO3Si3 004325-85-3 10 Abundance Scan 2888 (31.559 mln): 27288.D (-) m/ z 100.00% 73

5000 147 221 281 T-p-r Fl2t’11 31.20 31.40 31.60 31.80

miz-> 45 TMf 50 100 150 200 250 300 350 400 450 500 325.355.4014?% ! । 550 . m/z 147.00 38.23% Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 ' l 1 ' ‘ ‘ I ‘ ■ ■ ■ I ■ ■' ‘ I ' ' ‘ ■ I ‘ 147 31.20 31.40 31.60 31.80 221 281 327 m/z 221.05 21.73% 415 519 561 - L, m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance f . ;' Stlimr — <: 0 d puaalaniqng 73 147

31.20 31.40 31.60 31.80 5000 m/z 281.00 16.45% 45 190 219 1 mfe-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #53668:3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS ' 1 1 ■ ■ 1 ■ i ‘ 73 267 31.20 31.40 31.60 31.80 m/z 207.00 9.56% 5000 147

207 398 47 | miz-> 50 100 150 200 250 293.31. 300 350 400 450 500 550 AAWM 31.20 31.40 31.60 31.80

27288.D GCMS1126.M Mon Feb 04 15:23:46 2002 Page 13

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