GCMS analysis summary, sample AD27288, Dec 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JANO802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

32.94 0.62 ug/1 141894 Chrysene-dl2 32.84

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1,5,5,5- examethyl 384 C12H3604Si5 003555-47-3 38 2 1-Monolinoleoylglycerol imethylsi 498 C27H5404Si2 054284-45-6 38 3 1,1,1,5,7,7,7-Heptameth l-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 4 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 22 Abundance Scan 3038 (32.936 min): 27288.D (-) m/z 73.00 100.00% 73

5000 147 221 2811 355 TfTr PIT । *+ 106 327 [ 401 j9 32.60 32.80 33.00 33.20 111 Pjh IT 191 , 39 Pi i ' ■ i ■ ■ m/z 147.00 47.49% m/z-> 50 100 150 200 250 300 350 400 450 Abundance" #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 281 5000: 32.60 32.80 33.00 33.20 369 m/z 221.05 28.04%

m/z-> 50 • ■ 100 i 1 A29 1 150 200 250 300 t 338 J.......... 350 400 450 Abundance $6287! .Moncir '■: yigt ’ treothyigibe nem 73 N \...... . 32.60 32.80 33.00 33.20 207 5000 147 m/z 281.00 22.87% 34 103 281 395 482 miz-> 50 100 ' ' 150 200 250 300 ‘ 350 400 450 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t —4— juni 73 32.60 32.80 33.00 33.20 m/z 355.05 18.25% 147 5000 267 355 429 45 207

miz-> I ...... |[ TT118**Tr771T 50 100 150 200 L 250 300 350 1 1 ' 1*4-77 i ' 400 450 32.60 32.80 33.00 33.20 T

27288.D GCMS1126.M Mon Feb 04 15:23:51 2002 Page 14

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