NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26
Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS
Sample gems scan 12/20a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 12 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
32.94 0.62 ug/1 141894 Chrysene-dl2 32.84
Hit# of 5 Tentative' ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38
2 1 -Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 38
3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33
4 Silanamine, [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 22
Abundance Scan 3038 (32.936 min): 27288.D (-) m/z 73.0,0 100.00%
73
5000 147
221
281 355 —fTrTTutmmTtfrtf
106 401 429 32.60 32.80 33.00 33.20
39 191 J
11 11 r p#*r—4 Ai* 1 ■ • * i • •
i 327 I
■ • f ‘ 1 r • । • m/z 147.00 47.49%
miz-> 50 100 150 200 250 300 350 400 450
Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73 147
281
5000
32.60 32.80 33.00 33.20
369 m/z 221.05 28.04%
207 249. 1 , 338 .
miz-> 50 100
C
200
150 250 300 350 400 450
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
... A / \...
‘I**‘I**I***I***’}
207 32.60 32.80 33.00 33.20
5000 147 m/z 281.0.0 22.87%
34 103
281
395 .ao
482
m/z-> 50 100 150 200 250 300 350 400 450
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t —A— -
73 32.60 32.80 33.00 33.20
m/z 355.05 18.25%
147
5000 267
355 429
45 207
* ■ i *
.. I I.. j
**1**1***I**‘I‘ T 1d ! ! f । » I 1 i | « ! i I | > T TIBBnT
miz-> 50 100 150 200 250 300 350 400 450 32.60 32.80 33.00 33.20
27288.D GCMS0103.M Thu Jan 10 09:37:26 2002 Page 12
NYC-WTC_000018024
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