Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
NYC-WTC_000018005–000018025Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\JANO 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.
31.56 0.46 ug/1 106061 Chrys ene-dl2 32.84
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 42 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 3 3-(3-Hydroxypheny1) -3-hydroxypropio 398 C18H3404Si3 000000-00-0 23 4 Tris (trimethyj/silyl) borate 278 C9H27BO3Si3 004325-85-3 10 Abundance Scan 2888 (31.559 mln): 27288.D (-) m/z 73.0,0 100.00% 73
5000 147 281 221 ' l r ' 1 1 I 1 ' • 1 i ■ • **aan.a 429 31.20 31.40 31.60 31.80 45 TTMT 11174,11914., —32535401 410000. m/z 147.00 38.23% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 TI" 4 I ‘ ‘ • I ' 147 31.20 31.40 31.60 31.80 221 281 m/z 221.05 21.73% 327 415 519 561 t *’141*I*’’I****I’’’I***44— m/z—> 50 100 150 200 250 300 350 400 450 500 ’ 550 Abundance #30580: Ethanedioic acid, bisftrimetbyisily’) ester 73 147 31.20 31.40 31.60 31.80 5000 m/z 281.00 16.45% 45 i j 190 219 ■ ' i ' ■ ' ' I ■ ■ ' ■ i 1 1 ' ■ i ' ■ ‘ ■ i 1 ‘ ' 1 1 ‘ ' • ■ i ■ ■ ■ ■ i ■ ' ■ ■ i ■ ' ■ ■ i ■ * ' • i ■ ‘ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #53668:3-(3-Hydroxyphenyl)-3-hydroxyproplonic acid, tri-TMS 73 267 31.20 31.40 31.60 31.80 m/z 207.00 9.56% 5000 147
207 398
miz-> 47 | ■ • l • • • 1 I > • 1 • 1 > • • ■ i • < ' • f «“ 50 100 150 200 250 93. 31 300 . . MV 350 400 450 500 550 31.20 31'40 'step 31.80 1'
27288.D GCMS0103.M Thu Jan 10 09:37:21 2002 Page 11
NYC-WTC_000018023
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NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017980
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000017981
Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.
Filed in the same folder
NYC-WTC_000017989
Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.
Filed in the same folder
NYC-WTC_000017997
Laboratory report noting detection of 1,1,2,2-Tetrachloroethane in a water sample with no other non-target compounds.
Filed in the same folder
NYC-WTC_000018026
Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.
Filed in the same folder