NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GC/MS analysis results for sample AD30909, Jan 28 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
NYC-WTC_000018693–000018715Folder label: “GCMS X 12/19/01 A 1/2/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T.
34.37 1.04 ug/1 212509 Chrysene-dl2 33.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 32 2 2-Hexenedioicy4.cid, bis (trimethylsi 288 C12H2404Si2 055494-10-5 23 3 2-Ethyl-3-trimethylsilyloxy(trimeth 276 C12H2803Si2 000000-00-0 23 4 Butanoic aci , 3-methyl-2-[(trimeth 262 CllH26O3Si2 055124-92-0 23 Abundance Scan 3194 (34.369 min): 30909.D (-) m/z 72.95 100.00% 73
5000 147 — . 221 TTmr ■n-j-r 281 355 34.00 34.20 34.40 34.60 44 i 96 117 , 191 L 240 325 . [ 401 429 npmmpmmttmmtmmmnmpmmmmpm m/z 147.05 46.48% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance> #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(ti1met 73
7 147 _ . A. 5000 ■ ■ i ‘
281 34.00 34.20 34.40 34.60 45 369 26.81% 1 , 117 207 ._____ PLWI 249 . VrTTy+TTTfTTttpTTTp-rTTyTTTTp^ —angouanne 1>Il|1I1IJI. | > i I > | i < i , 11 ■ i . | . H i । i , i . 11 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #40777 2-Hexenedioic acid, bis(trimethylsily!) ester, (E)- 73 * I r I I » I • » f » I I ' ■ ■ i ■ ' ■ ■ i • 34.00 34.20 34.40 34.60 5000 m/z 281.00 17.03% 147 ............................................. 45 । , 244 273 Tmmm"menm —112 mmN"amT TWIWWOTTTTpTM]]] m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #38736:2-Ethyl-3-trimethylsilyloxy(trimethylsilyi)butyrate A AA AAAMACi , ITTAPW, 73 34.00 34.20 34.40 34.60 117 m/z 355.05 ..................... / 12.88% 5000 147 45
—’0—Il—0""EIB8899188 l mH ... 191 232261....................... m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 34.00 34.20 34.40 34.60 ' ‘ ‘ '
30909.D GCMS1126.M Fri Jan 25 11:40:54 2002 Page 13
NYC-WTC_000018713
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