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GC/MS analysis results for sample AD30909, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.

NYC-WTC_000018693–000018715

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 1-Monolinoleoylglycerol trimet Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

36.71 0.70 ug/1 81677 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 42 2 3-Isopropoxy-lyl,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23 3 2-Butenoic acid, 3-methyl-2-[ (trime 260 CllH24O3Si2 055044-79-6 17 4 3,7-Dioxa~2/6-disilanonane, 2,2,8,8 220 C9H2402Si2 017887-80-8 17 Abundance Scan 3449 (36.710 min): 30909.D (-) m/z 73.0,0 100.00% 73

147 5000 221 281 355 ■ ‘ i ‘ • i ■ • ■ ■ i ■ ' ‘ 1 i ' ■ • ■ i

•4 39 36.40 36.60 36.80 37.00

miz-> 1' n > 1 4 1’1 ■ 50 100 150 1934 200 250 300 350 400 450 500 550 m/z 147.00 !52.93% Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 IMYT 34 i 36.40 36.60 36.80 37.00 103 | m/z 221.0 29.55% 281 395..... 482. 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503; 3-lsopropoxy1.1.1.7.7.7-hexamethyl-3,5,5-tris(trim 73 --A 36.40 36.60 36.80 37.00 5000 m/z 355.05 16.09% 147 221 281 ' ' I ' ‘ ‘ ' I ‘ ‘ ' I 1 1 1 1 I 1 '■ 1 1 1 1 1 ' 1 r ' 350 327 ..... 415. , .... 519 561 400 450 ' 500 ' ‘ 550 ‘ miz-> 50 100 150 200 250 300 Abundance #71699:2-Butenoic acid, 3-methyl-2-[(trimethylsilyl)oxy]-, ■ ‘I • 1 1 ' I 147 36.40 36.60 36.80 37.00 m/z 281.00 14.83% 73 5000

45 245 217 | — , . 113,7 . 1 I I 11 I I I I I IIII I • » I I I » ! I I I l'"l 'I J I I I I I I I I IT m/z—> 50 100 150 200 250 300 350 400 450 500 550 36.40 36.60 36.80 37.00

30909.D GCMS1126.M Fri Jan 25 11:41:03 2002 Page 15

NYC-WTC_000018714

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NYC-WTC_000018714Source: NYC Law Department, mirrored locally

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