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GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036773
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method :. C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************** * * ************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

36.72 10.25 ug/1 3914390 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 39 2 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 25 3 N-BenzhydryLidene-1-(2,4,6-trimethy 343 C24H25NO 089839-57-6 22 4 3,3-Diphenyl-2-[1-(2,4,6-trimethylp 343 C24H25NO 075326-12-4 22 Abundance 2 Scan 3450 (36.720 min): 29522.D.(-) " —T 1 m/ z 73

147 5000 221 281 355 36.40 36.60 36.80 37.00 0+1 145 —T 96 117 TIH 168191 38,191 1——251 —42741 1--19I 401 429 m/z 147.00 56.48% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether t 73

| 207 5000 147 • ■ । • ■ • ■ । ■ ■ ■ t • • ■ 1 i 36.40 36.60 36.80 37.00 34 103 281 m/z J 36.72% miz-> K 50 100- 150 200 250 A 300 350 400 450 482

'Abundance #71006: Ethanedioic acid, bis(trimethy!sily!) ester 1 • 73

147 36.40 36.60 36.80 37.00 5000 m/z J 20.15%^ 45 1 117 | 190 219 TiI- m/z-> 50 100 150 200 250 300 350 400 450 Abundance #48514: N-Benzhydrylidene-1-(2,4,6-trimethylphenyl)ethylami 147 36.40 36.60 36.80 37.00 m/z J 17.30%^ 5000-

........ 182 ......... 312 343 ......... m/z-> 50 100 150 200 250 300 350 400 450 36.40 36.60 36.80 37.00

29522.D GCMS1126.M Fri Jan 18 16:49:20 2002 Page 16

NYC-WTC_000036773

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NYC-WTC_000036773Source: NYC Law Department, mirrored locally

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