GCMS analysis results for sample AD29522, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 17 1-Monolinoleoylglycerol trimet Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

38.01 6.11 ug/1 2335160 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 39 2 Silanamine, X- [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 30 3 Ethanedioic/acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 25 4 Propanoic /acid. 2-OXO-3-(trimethyls 232 C9H20O3Si2 Abundance Scan 3591 (38.015 min): 29522.0 (-) 73 m/ z 70 055887-51-9 25

147 5000 221 281 355 TT 191 1 , । 251 „ [ 302 327, | 37.60 37.80 38.00 38.20 38.40 I 0—r 11- 45 96 117 PI’T । TndT TIT yynr TTI । TTdnyt 401 429 1 -1 1 T 1 i 1 m/ z 147.00 57.57% miz- 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 37.60 37.80 38.00 38.20 38.40 I 34 103 । 281 m/z 221.05 37.39% - 395 482 I , m/z—> 50 100 150 200 250 300 350 400 450 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsily!)oxy] 73 1 281 T-j-i-i-i-i-r । । । 37.60 37.80 38.00 38.20 38.40 209 ! 5000 45 251 | m/z 281.00 19.55% > I . 1791 TI । 125147i | il i................... ,m/z-> 50 100 150 200 250 300 350 400 450 ) Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester TT ■ i ' ■ 73 37.60 37.80 38.00 38.20 38.40 m/z 355.0, 16.34% 147 5000

45 1 1 117 190 219.................................................................... ■ i ■ m/z-> 50 100 150 200 250 300 350 400 450 37,60 37.80 38.00 38.20 38.40

29522.D GCMS1126.M Fri Jan 18 16:49:25 2002 Page 17

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