GCMS analysis results for sample AD27232, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1201\27232.D Vial: 12 Acq On 13 Dec 2001 1:18 am Operator: GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 2 t

R.T. EstConc Area Relative to ISTD R.T.

3 9.68 0.42 ng/uL 84614 Perylene-dl2 37.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monol inoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 38 2 9,12,15-Octadecatrienoic acid, 2,3- 496 C27H5204Si2 055521-22-7 10 3 3-Isopropoxy-1,1 1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 9 4 Silanamine, N- ,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 4 Abundance 7 Scan 3799 (39.679 min): 27232.D (-) m/z 73.05 100.00% 73 147 5000 221 281 A AMA — 355 _ — — 39.40 39.60 39.80 40.00 44 ..... 1 m/z 147.10 64.10%

A > ■ ■ i ■

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147 TT I I ‘IETT 1 1 39.40 39.60 39.80 40.00 34 103 281 m/z 221.05 4 2.94%

m/z-> .. 150 1 _ 200 250 300 350 325,400.....450,4?2500 , . 550 50 100 'Abundance #58836: 9.12.15-Octadecatrienoic acid. 2,3-bis[(trimethylsi 73 147 TL.F 220 39.40 39.60 39.80 40.00 5000 109 m/z 281.10 32.48% 191 281 249 742- m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 39.40 39.60 39.80 40.00 m/z 355.05 21.07% 5000 147

221 281 327 -— 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450 500 550 39.40 39.60 39.80 40.00

27232.D NP112701.M Fri Dec 14 10:07:51 2001 Page 2

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