DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30709.D Vial: 47 Acq On : 30 Dec 2001 4:24 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M '(RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

35.57 1.17 ug/1 361227 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerbl trimethylsi 498 C27H5404Si2 054284-45-6 45 2 Ethanedioic acid, bis(trimethylsily 234 C8H1804Si2 018294-04-7 38 3 3-(3-Hydroxyphenyl)-3-hydroxypropio 398 C18H3404Si3 000000-00-0 38 4 1,2-Benzenedicarboxylic acid, bis (t 310 C14H2204Si2 002078-22-0 37 Abundance Scan 3325 (35.569 min): 30709.D (-) m/z 73.00 * 100.00% 73

147 5000 221 281 ggg 35.20 3540 35.60 35.80 ' 45 TT 95 117. , , 1911 , 249 „ j L 327, L 401 429 m/z 147.00 50.51% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000- 147 35.20 35.40 35.60 35.80 34 103 281 m/z 221.0,5 31.45% i ‘ • ■ । ■ 14 । [i 010%5.... 482 Mz-> 50 100 150 200 250300 350 400 450 Abundance #71005. Ethanediolc acic bisttimth . tl 73 ■ • l ' 147 35.20 35.40 35.60 35.80 5000 m/ Z 281.00 17.50% 45 117 190 219 । m/z-> 50_____ 100 150 200 250 300 350 400 450 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS 73 267 35.20 35.40 35.60 35.80 m/z 207.00 14.63% 5000 147

207 398 47 - TI 293 . . 341 . m/z~> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80

30709.D GCMS1126.M Mon Jan 28 11:33:36 2002 Page 13

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