Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
NYC-WTC_000017703–000017723Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2 701\30425.D Vial: 5 Acq On : 27 Dec 2001 3:04 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 1-Monolinoleoylglycerol trimet Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 35.57 0.50 ug/1 90153 Perylene-dl2 37.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404S12 054284-45-6 39 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 3 1,2-Benzenedicarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 23 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 20 Abundance Scan 3325 (35.567 mln): 30425.D (-) m/z 72.95 100.00% 73
147 5000 221 281 A5E
miz-> —4450 94 119 100 150 , 1914 200 .13278... 42°. 250 300 350 400 450 ‘ I * • ‘ ‘ I 1 ‘ ‘ 1 1 1 1 * 1 I 1 1 1 1 1 r 35.20 35.40 35.60 35.80 m/z 147.00 54.96% Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73
5000 147 207 n 4. ,/, lomapelai AA 35.20 35.40 35.60 35.80 34 103 m/z 221.05 31.82%
m/z~> 4 ■ i 50 • ■ 1 1 T-IT 100 150 ‘266 ‘ 250 300 I. , 21... .. 350' 395 - 400 450 482
Abundance #71005: Ethanedioic add. bis trimethylsilyl) ester 73
147 35.20 35.40 35.60 35.80 ' ' 5000 m/z 281.00 18.94% 45 117 , 190 219 • ‘ i • ' ■ ■ i ■ • ■ ■ I 1 • ' 1 i • ‘ 1 1 1 ' ‘ ' • i ■ ‘ ■ ■ i ‘ ■ ■ ■ i ■ ‘ ■ ■ i ' ‘ m/z-> 50 100 150 200 250 300 350 400 450 Abundance #72972: 1,2-Benzenedicarboxylic acid, bis(trimethyisily!) e 147 35.20 35.40 35.60 35.80 ‘ m/z 355.05 15.08% 73 5000 / 45 295 ; , . 193 • I ‘ * 111 . 110 , ........I......................... . ■ i ■ ' ■ • I 1 ■ ■ ■ i ■ ■ 1 ■ i ■ • ' • i ' ' ‘IT miz-> 50 100 150 200 250 300 350 400 450 35.20 35.40 35.60 35.80
30425.D GCMS1126.M Wed Jan 02 11:04:36 2002 Page 13
NYC-WTC_000017722
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NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017649
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000017650
Laboratory log recording extraction parameters and sample counts for environmental samples processed in December 2001.
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NYC-WTC_000017654
Document showing calibration results for GCMS analysis of volatile organic compounds on December 27, 2001.
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NYC-WTC_000017658
Laboratory report documenting gas chromatography-mass spectrometry reference material analysis conducted on December 31, 2001.
Filed in the same folder
NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
Filed in the same folder