Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
NYC-WTC_000018470–000018491Folder label: “GCMS X 12/18/01 A 12/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\DEC2701\30645.D Vial: 53 Acq On : 30 Dec 2001 10:14 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 1-Monolinoleoylglycerol trimet Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
35.57 1.30 ug/1 315356 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoyiglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 38 2 2-Methoxyphenylpyruvic acid, di-TMS 338 C16H2604Si2 000000-00-0 32 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 Propanoic acid, 2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 23 Abundance Scan 3325 (35.570 mln): 30645.D (-) m/ z 73.00 100.00% 73 __
147 5000 221 ■ i * ■ 400 45 T ■ • 111 r 4, .1934 .96100117,‘ 150 ‘260 _ 249.,281. 327 355 J • 401 429 35.20 35.40 35.60 35.80 m/z 147.00 50.67% mlz-> 50 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 ....................... __ 207 5000 147 35.20 35.40 35.60 35.80 34 103 m/z 221.05 31.08% 281 1 395 ............................. ......................... 482 1 • i ■ ■ ■ • I ' • 1 ■ IT ./tamegog 450’ ‘ ‘ ' m/z-> 50 100 150 200 250 300 350 400 Abundance #47880:2-Methaxyphenylpyruvic acid, di-TMS 147 35.20 35.40 35.60 35.80
"T 5000 73
267 , 47 , j j............ 207 307 ' i • • ' ‘ i ' ■ i ■ ■ ' ■ i ■ • ■ ■ i ■ ' miz-> 50 100 ' 150 ' ' 200 250 300 350 400 450 Abundance #71006: Ethanedioic acid, bis(trimethylsily!) ester • • • I * • 111 » * . J * 73 35.20 35.40 35.60 35.80
5000
m/z-> 45 117 • 'I ‘ ' ' • i ' ■ ' ' i ■ 50 100 147
, 190 219 150 ’200’ '250' ' 300 ’ 350 400 450 X. ‘ I ‘ ‘ ‘ > I 1 I f ' I I 1 ‘ 1 I 35.20 35.40 35.60 35.80 ■ ■ i ■
30645.D GCMS1126.M Fri Feb 01 10:53:34 2002 Page 15
NYC-WTC_000018489
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NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018416
Single-page document containing GCMS data or metadata associated with the WTC site in December 2001.
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NYC-WTC_000018417
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018436
Laboratory report documenting GCMS calibration data for sample AD30643 conducted on February 1, 2002.
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NYC-WTC_000018440
Laboratory report documenting GCMS reference analysis of sample AD30643 conducted on February 1, 2002.
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