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GC/MS calibration data for sample 28323, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018519–000018545

Folder label: “GCMS X 12/18/01 A 12/30/01

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Scanned page image, NYC-WTC_000018541
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 1-Monolinoleoylglycerol trimet Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

35.57 5.26 ug/1 1356790 Perylene-dl2 37.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 45 2 3-Isopropoxy-1, 1,1,7, 7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 34 3 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32 4 N-Benzhydrylidene-1-(2,4,6-trimethy 343 C24H25NO 089839-57-6 27 Abundance Scan 3325 (35.572 min): 28323.D (-) m/z 73.00 1 00.00% 73

147 5000 221 — ■ । rm 'i vi । i । । 281 355 ■ l * 1 327, 1 401 49 35.20 35.40 35.60 35.80 36.00 45 1 • 1 i 1 ‘ 17 117 , * 191[ , 24944,4 -ITT —me m/z 147.00 51.42% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73 207 5000 147 1 • l ‘ 35.20 35.40 35.60 35.80 36.00 34 103 I 281

miz-> 50 100 150 200 250 300 350 395, 400 ,482. 450 500 550 Abundance #60503: 3-Isopropoxy-1.1.1 jy -hexamett »-3,5,5-tris(trim 73

35.20 35.40 35.60 35.80 36.00 5000 m/z 281.00 18.38% 147 221 281 327 415 519 561 m/z-> 50 100 150 200 250 300 350 400 450" 500 ’ 550 Abundance #71005: Ethanedioic acid, bis(trimethylsily!) ester IBRTpBBtnTPrprTrerm 73 35.20 35.40 35.60 35.80 36.00 m/z 355.05 14.86% 147 5000

45 [ 11 117 . 219 190 cto i r '"i II[a I r । । vi 1j.it > | • । T"1 । .... t | I r | > i i i | rr miz-> 50 100 150 200 250 300 350 400 450 500 550 35.20 35.40 35.60 35.80 36.00

28323.D GCMS1126.M Wed Feb 06 13:02:41 2002 Page 17

NYC-WTC_000018541

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NYC-WTC_000018541Source: NYC Law Department, mirrored locally

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