DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

36.72 1.02 ug/1 273382 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 50 2 1,2-Benzenediaarboxylic acid, bis(t 310 C14H2204Si2 002078-22-0 32 3 Propanoic acid, 2-oxo-3-(trimethyls 232 C9H20O3Si2 055887-51-9 25 4 Ethanedioic cid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 Abundance Scan 3450 (36.719 min): 30707.D (-) m/z " 100.00% 73

147 5000 221 281 355 36.40 36.60 36.80 37.00 I 45 1' i '■ 95 117 li ' ' M" ' . , ,191 ,253, । T4I i 327 [ ii rII 401 429 ’ r * ■ ■ *T m/z 147.00 54.91% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73

207 --=== 5000 147 151“ FT 36.40 36.60 36.80 37.00 34 103 281 m/z 221.05 33.19%

m/z-> 50 100150 200 — k, , , 250 300 350 395 i

400 ,

450 482

Abundance #72972: 1.2-Penzenedicarboxylic add bisttrimethvisily!) e i 147 I I 73 1 1 i ■ ■ ' 1 i i 36.40 36.60 36.80 37.00 i 5000 m/z 281.00 20.01% 45 295 119 , 193 221 । m/z—> 50____ 100 150 200 250 300 350___ 400 450 Abundance #30222: Propanoic acid, 2-oxo-3-(trimethylsilyl)-, trimethy 1TI i ■ ■ ' ■ i 147 36.40 36.60 36.80 37.00 73 m/ z 207.00 15.89% 5000 45 217 117 . . 189 J.......................................................... ' 'i ■ ' m/z-> 50 100 150 200 250 300 350 400 450 36.40 36.60 36.80 37.00 '

30707.D GCMS1126.M Mon Jan 28 11:24:53 2002 Page 16

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