NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30707.D Vial: 41
Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS
Sample : GC/MS SCAN 12/18 Inst : GC/MS 209
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10
R.T. EstConc Area Relative to ISTD R.T.
35.57 1.88 ug/1 504016 Perylene-dl2 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38
2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36
3 dl-Xylitol, cyclic 2/3- (phenylboron 238 C11H15BO5 074793-46-7 27
4 N-Benzhydrylidene-1/(2,4,6-trimethy 343 C24H25NO 089839-57-6 27
Abundance ..... Scan 3325(35.572 min): 30707.D (-)........ m/z 73.00 100.00%
73
147
5000-
221
TTT
145, .249 281L 325 355
. 35.20 35.40 35.60 35.80 36.00
[ 401 429
4 , 112 „ 4
43,
ITII fl l ] 1-1 1I I I “I 1111 T1*ITTP m/z 147.00 50.36%
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet
73
147
—। T r । . . । i — । 1e- r i
5000
281 35.20 35.40 35.60 35.80 36.00
45 ! 369 m/z 221.05 30.51%
1
' IBU
117 . , 20/ 249.............. |............
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #60503: 3-sopropoxy-1 .1 ,1 z 7 /-hexamethyl-3,5,5-tris(trim
73
■ ‘ l '
35.20 35.40 35.60 35.80 36.00
5000 m/z 281.00 17.53%
147
m/z->
.......
50 _ 100__ 150
.........
200 __ 250 __ 300 350
415. 450
400
... __ 500
519.561
550
Abundance #31417: di-Xylitol, cyclic 2,3-(phenylboronate) 00000 ■ ■ 1 i ' • 1 ■ i ■ ' ■ ■ i ■
147 35.20 35.40 35.60 35.80 36.00
m/z 207.00 13.12%
61
5000
104
31 177
I I 1 । 207 238 ...................
m/z-> 50 100 150 200 250 300 350 400 450 500 550 35.20 35.40 35.60 35.80 36.00
30707.D GCMS1126.M Mon Jan 28 11:24:48 2002 Page 15
NYC-WTC_000004457
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