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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004457
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.57 1.88 ug/1 504016 Perylene-dl2 37.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 38 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 36 3 dl-Xylitol, cyclic 2/3- (phenylboron 238 C11H15BO5 074793-46-7 27 4 N-Benzhydrylidene-1/(2,4,6-trimethy 343 C24H25NO 089839-57-6 27 Abundance ..... Scan 3325(35.572 min): 30707.D (-)........ m/z 73.00 100.00% 73

147 5000- 221 TTT 145, .249 281L 325 355 . 35.20 35.40 35.60 35.80 36.00 [ 401 429 4 , 112 „ 4 43, ITII fl l ] 1-1 1I I I “I 1111 T1*ITTP m/z 147.00 50.36% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 —। T r । . . । i — । 1e- r i 5000 281 35.20 35.40 35.60 35.80 36.00 45 ! 369 m/z 221.05 30.51% 1 ' IBU 117 . , 20/ 249.............. |............ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-sopropoxy-1 .1 ,1 z 7 /-hexamethyl-3,5,5-tris(trim 73 ■ ‘ l ' 35.20 35.40 35.60 35.80 36.00 5000 m/z 281.00 17.53% 147

m/z-> ....... 50 _ 100__ 150 ......... 200 __ 250 __ 300 350 415. 450 400 ... __ 500 519.561 550 Abundance #31417: di-Xylitol, cyclic 2,3-(phenylboronate) 00000 ■ ■ 1 i ' • 1 ■ i ■ ' ■ ■ i ■ 147 35.20 35.40 35.60 35.80 36.00 m/z 207.00 13.12% 61 5000 104 31 177

I I 1 । 207 238 ................... m/z-> 50 100 150 200 250 300 350 400 450 500 550 35.20 35.40 35.60 35.80 36.00

30707.D GCMS1126.M Mon Jan 28 11:24:48 2002 Page 15

NYC-WTC_000004457

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NYC-WTC_000004457Source: NYC Law Department, mirrored locally

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