GC/MS calibration data for sample 28323, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 19 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

38.01 2.07 ug/1 532503 Perylene-dl2 37.11

Hit# of 5 Tentative” ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1,1, 5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 37 2 Silanamine, N-12,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 27 3 dl-Xylitol, cyclic 2,3-(phenylboron 238 C11H15BO5 074793-46-7 27 4 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 25 Abundance Scan 3591 (38.014 min): 28323.D (-) m/z 73" 100.00% 73

147 5000 221 281 355 • i • • > • i ■ ■ 37.60 37.80 38.00 38.20 38.40 55 96 119 T" Tpnt mhm TL’T T 4+249,+4447+327,+44444Q1.43, 191 m/z 147.00 56.73% m/z-> 20 40 60 80 100120140160180200 220240260280300 320 340 360 380 400 420 " Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

m/z-> 5000

45 , I’*’—I—tttdt"ad31 117 1 207 249 281

’3Umm“nn—nnu—"umam—ng—nr ’’’I’’’I’I——CD—WUB9—AA1’48114 20 40 60 80 100120140160180200220240260 280 300 320 340 360 380400420 369 m/z "NT —KudnBTTeuT 37.60 37.80 38.00 38.20 38.40

Abundance #39584: Silansmine. N-(2,6-dimethyl-4-litrmetnyisilylg v; 73 281

5000 45 209 251 I

m/z "T 37.60 37.80 38.00 38.20 3840

147 179 125 147 1

TTMImmmmmmpTmmmmp J(».» ________________________ j j j ।. j 11 u j j j.»11 rn 11 j 11111 j 11 n n ) j i m/z-> 20 40 60 80 100120140160180200220240260280300320 340360 380400 420 Abundance #31417: dl-Xylitol, cyclic 2,3-(phenylboronate) 147 37*60 37.80 38.00 38.20 38.40 m/z 355.0 15.96% 61 5000 104 31 177 — — ............... i „ — 238 ..................................... _............. 44,14111411144 • • 1 ‘ * m/z-> 20 40 60 80 100 120140160180 200 220 240 260280 300 320 340 360 380 400 420 ' 37.60 37.80 38.00 38.20 38.40

28323.D GCMS1126.M Wed Feb 06 13:02:51 2002 Page 19

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