GC/MS calibration data for sample 28323, Dec 2001

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Data File : C:\HPCHEM\1\DATA\DEC2701\28323.D Vial: 63 Acq On : 30 Dec 2001 8:55 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 20 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

39.58 1.16 ug/1 298372 Perylene-d12 37.11

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 33 2 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 22 3 dl-Xylitol,cyclic 2,3-(phenylboron 238 C11H15BO5 074793-46-7 14 4 Silanamine, N-[2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 14 Abundance { Scan 3762 (39.584 mln): 28323.D (-) m/z 73.00 100.00%

A 73 147

5000 221 281 355 429 39.20 39.40 39.60 39.80 40.00 Tr 42 , 97 119 | J “•f ‘i '| । n । 191-— PI 325 1,440144 m/z 147.00 65.46% m/z-> 50 100 150 200 :250 300 350 400 Abundance #56714:1,1,1,5'7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 147 5000 267 ’ 11241.1. urimmmmnne 355 429 39.20 39.40 39.60 39.80 40.00 207

m/z-> 45 I 50 .... :___ ______ I,...... 100 150 200 250 300 350 400 4— Abundance t7100ht Ethanedicic acid, bisprimeinyisily! unr* 73

147 39.20 39.40 39.60 39.80 40.00 5000 m/z 207.00 23.61% 45 117 , 1 190 219 K m/z-> 50 100 150 200 250 300 350 400 Abundance #31417: dl-Xylitol, cyclic 2,3-(phenylboronate) 147 39'20 39.40 39.60 39.80 40.00 m/z 281.00 20.55% 61 5000 104 31 177

' ■ 1 I 1 297, 238 m/z-> 50 100 150 200 250 300 350 400 39.20 39.40 39.60 39.80 40.00

28323.D GCMS1126.M Wed Feb 06 13:02:56 2002 Page 20

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